关键技术参数：

l  三路气体，采用MFC质量流量计控制流量，气体流量计精度±1% F.S，准确度±1% F.S，耐压16 MPa，可在线动态配气、脉冲反应以及瞬态气体切换，带数字模块；

l  一路液体，高压输液泵流量控制流量，设定范围0.001~4.999 ml/min、最大压力42 MPa、流量准确度：±0.5%、流量精度：±0.2%；液体柱塞泵泵头带加热功能，可设定保温温度室温~1200℃，温度控温精度<±1 ℃；

l  液体柱塞泵泵头以及液体进口管道缠绕加热带进行保温；液体原料罐体积500 ml，外置加热套，温度范围：室温~300 ℃，温度控温精度<±1 ℃，液体出料口设置过滤头；

l  管式炉：开式保温反应炉，采用纤维烧结炉膛、电炉丝加热。耐温性能优越、加热稳定和温度均匀。内置耐高温恒温导热块，温度控制精确，程序控温线性度高，反应炉温度：室温~1200；恒温区120 mm；程序升温速率：0.5~90 ℃/min；

l  双热电偶进行温度控制和显示，测温显示热电偶从上往下插入催化剂上方；

l  配备耐高温高压反应管，外径~16 mm，内径~10 mm，采用不锈钢弧面硬密封的密封方式，配催化剂支撑内衬，催化剂装填量~12 ml；

l  混合器内置导流板，在气体流动过程通过气体反复的膨胀和收缩来实现气体的均匀混合，实现在线配气；

l  反应炉出口配备取样针型阀，连接至色谱仪的管道全程保温，微调该取样针型阀实现少量产物全保温状态下进色谱仪分析，大量产物进入下端的气液分离器（冷凝器和收集器）中进行冷凝和气液分离；冷凝器和收集器为双层结构，内部有冷凝盘管，外层通入冷凝液进行降温，以对反应产物进行气液分离；冷凝器外体积~200 ml，收集器外体积~250 ml，内体积~100 ml，外接循环制冷泵，温度-10 oC~RT；

l  每段炉均采用程序升温控温表，配备串级功能及双输入模式，取通道中测量值低或者高的主控测量值；

l  配电脑程序软件，能控制反应炉温度和气体流量，显示反应温度，并实时记录温度和流量曲线；并可以编辑加热器加热、流量设置等动作，能够实现一键运行；另外软件上具有温度过高、压力过高、氢气泄露情况下，整体设备断电的断路控制处理功能；配备完整的测试软件，测试程序可根据客户要求进行编程，并可完成测定结果的自动化生成，与此同时可对已测定结果进行数据后处理；

l  带有注射口，注射垫片可更换，方便定量；

l  采用铝型材框架、铝合金面板以及组合式方式，美观大气，客户可自行进行部分调整。

Key technical parameters:

l  The three gas channels are controlled by an MFC mass flow meter, with an accuracy and precision of ± 1% F.S, a pressure resistance of 16 MPa, and support for online dynamic gas distribution and other functions.

l  The liquid is controlled by a high-pressure infusion pump, with a flow range of 0.001~4.999 ml/min, a maximum pressure of 42 MPa, an accuracy of ± 0.5%, and an accuracy of ± 0.2%.

l  The pump head and pipeline are equipped with heating function, and can be set to room temperature~1200 ℃. The liquid raw material tank is equipped with an external heating sleeve, with a temperature range of room temperature to 300 ℃.

l  The tube furnace adopts a fiber sintering furnace, with precise temperature control and a programmed heating rate of 0.5~90 ℃/min.

l  The dual thermocouple system precisely controls and displays the reaction temperature, ensuring the accuracy of the experiment.

l  Equipped with a high-temperature and high-pressure reaction tube with an outer diameter of 16mm and an inner diameter of 10mm, using stainless steel curved hard sealing, and a catalyst loading capacity of approximately 12ml.

l  The mixer is equipped with a built-in guide plate to achieve uniform gas mixing and online gas distribution. The outlet of the reaction furnace is equipped with a sampling needle valve, and the pipeline connected to the chromatograph is fully insulated. The product can be finely adjusted to enter the chromatograph or gas-liquid separator.

l  The separator has a double-layer structure, which includes a condensing coil. The outer layer is cooled by condensate, and an external refrigeration pump is connected. The temperature range is -10 ℃ to room temperature.

l  Each section of the furnace adopts a programmed temperature control meter, which supports cascade function and dual input mode to ensure stable and controllable experimental processes.

l  Equipped with computer software to control the temperature and gas flow of the reactor, record curves, and achieve one click operation. Equipped with safety power-off function, the testing software can be customized and programmed to automatically generate and process measurement results.

l  Equipped with an injection port, the injection gasket can be replaced for easy quantification;

l  Adopting aluminum profile frames, aluminum alloy panels, and combination methods, customers can adjust them themselves.

该装置包括控制系统、进料系统、反应系统、分离系统等。

工艺流程：

原料油从原料油罐中经液体过滤器过滤后由计量泵抽出，升压后和新氢进行混合。新氢经过稳压阀稳压后，由MFC（质量流量控制器）控制流量后和原料油混合。

油氢气混合物进入反应器的预热段，预热至反应温度后进入恒温段和催化剂接触进行反应，反应产物经冷凝器冷凝后，进入热高分进行气液分离。

气相产物经高压缓冲罐、再经过压力调节阀控制系统压力后排放，经碱洗、计量后排空；高压分离器液相产物经过液位控制阀控制液位后进入产品罐，产品罐放出的富气汇合至高分尾气，和高分尾气一起经过碱洗、计量后排空。

The device includes a control system, feeding system, reaction system, separation system, etc.

Process flow：

After filtering, the raw oil is pressurized and mixed with new hydrogen for stabilization and metering.

Preheat the mixture of oil and hydrogen to the reaction temperature, react with the catalyst, condense, and then undergo gas-liquid separation through thermal separation.

The gas-phase products are discharged after buffering and pressure regulation, and then discharged after alkali washing and metering; The liquid phase product is controlled to enter the product tank at the liquid level, and the rich gas is collected and discharged through alkaline washing of the high concentration tail gas.

关键技术参数：

催化剂装填量：20mL-40mL；

设计压力：20 MPa；使用压力：8-18 MPa；

设计温度：~550℃；使用温度：~500℃；

空速：0.3~3.0 h-1；

氢油比：300~1000；

氮气和氢气两路气体，质量流量计品牌为Brooks；

原料计量泵为高压隔膜泵，采用防爆变频电机，品牌为LEWA、ELDEX等进口品牌；

球阀、针阀及单向阀等阀件的品牌为Swagelok；

减压阀、背压阀及稳压阀的品牌为TESCOM等进口品牌；

原料罐及产品罐配套电子秤，可进行物料衡算，电子秤精度为0.1 g；

加热炉方式：可开启式电加热炉；

要求自动化控制，在组态软件中要实现气体流量、液体流量、程序温度的调节和记录，相关数据可回溯与导出。

配备控制电脑，系统I5以上，内存8G以上，23寸显示器。

控制硬件采用honeywell的HC900的DCS系统

主要配置

油品高值化固定床装置：1套；

控制电脑：1台。

附属设备及备品备件

备用反应器1根；

密封圈、阀门2个，三通3个，直通2个，管线4米，工具箱一套。

Key technical parameters:

Catalyst loading capacity: 20mL-40mL;

Design pressure: 20 MPa; Operating pressure: 8-18 MPa;

Design temperature:~550 ℃; Operating temperature:~500 ℃;

Airspeed: 0.3~3.0 h-1;

Hydrogen oil ratio: 300-1000;

Nitrogen and hydrogen are two gas channels, and the mass flow meter brand is Brooks;

The raw material metering pump is a high-pressure diaphragm pump, explosion-proof variable frequency motor, LEWA, ELDEX and other brands;

The brand of valve components such as ball valves, needle valves, and one-way valves is Swagelok;

The brands of pressure reducing valves, backpressure valves, and pressure stabilizing valves are imported brands such as TESCOM;

The raw material tank and product tank are equipped with electronic scales, with an accuracy of 0.1 g;

Heating furnace method: openable electric heating furnace;

Automated control, relevant data can be traced and exported.

Equipped with a control computer, system I5 or above, 8GB or more of memory, and a 23 inch display.

The control hardware adopts Honeywell's HC900 DCS system.

Main configurations

One set of high-value fixed bed equipment for oil products;

Control computer: 1 unit.

Auxiliary equipment and spare parts

One spare reactor;

Two sealing rings, two valves, three tees, two straight pipes, a 4-meter pipeline, and a set of toolbox.

案例：

螺杆式生物质连续热解反应器结构图：

本设备的应用是将木质纤维素、农业废弃物等转化为清洁能源。

下图为50kg螺杆式生物质连续热解反应器，最高使用温度为600℃，不锈钢材质。

反应器的长度、内径以及螺杆的转速取决于生物质的停留时间。

应用领域包括：

纤维素，木质素，塑料，污泥，生物质，石墨，岩石，低阶煤，油泥，低密度聚乙烯，水基泥浆，废料，城市生活垃圾。

Structural diagram of screw biomass continuous pyrolysis reactor:

The application of this equipment is to convert lignocellulose, agricultural waste, etc. into clean energy.

The picture below shows a 50kg screw biomass continuous pyrolysis reactor with a maximum operating temperature of 600°C and made of stainless steel.

The length, inner diameter and screw speed of the reactor depend on the residence time of the biomass.

Application areas include:

Cellulose, lignin, plastic, sludge, biomass, graphite, rock, low-rank coal, sludge, low-density polyethylene, water-based slurry, waste materials, municipal solid waste.

小试热解反应器现场图：

本设备的应用是将木质纤维素、农业废弃物等转化为清洁能源。

下图为小试用热解反应器，最高使用温度为1000℃，不锈钢材质。

Site diagram of small-scale pyrolysis reactor:

The application of this equipment is to convert lignocellulose, agricultural waste, etc. into clean energy.

The picture below shows a small trial pyrolysis reactor with a maximum operating temperature of 1000℃and made of stainless steel.

中试热解反应器现场图：

本设备的应用是将木质纤维素、农业废弃物等转化为清洁能源。

下图为20kg/小时的连续螺杆式热解反应器。反应器温度PID控制器，5个加热区分区控温。

Site diagram of pilot pyrolysis reactor:

The application of this equipment is to convert lignocellulose, agricultural waste, etc. into clean energy.

The picture below shows a 20kg/hour continuous screw pyrolysis reactor. Reactor temperature PID controller, 5 heating zones zone temperature control.

生物质焙烧装置现场图：

焙烧是对生物质进行初步热化学处理以改善其燃料特性的一种技术。

本装置用于研究禽畜粪便加工成环保燃料的最佳操作条件。实验过程如下：1kg生物质颗粒批量加入反应器中，气相(氮/蒸汽)的流速为0.68-0.8 m/s。工作温度250℃/300℃/350℃，工作压力0.2MPa。

Site diagram of pilot pyrolysis reactor:

The application of this equipment is to convert lignocellulose, agricultural waste, etc. into clean energy.

The picture below shows a 20kg/hour continuous screw pyrolysis reactor. Reactor temperature PID controller, 5 heating zones zone temperature control.

Site diagram of biomass roasting device:

Torrefaction is a technique for preliminary thermochemical treatment of biomass to improve its fuel properties.

This device is used to study the optimal operating conditions for processing livestock manure into environmentally friendly fuel. The experimental process is as follows: 1kg biomass particles are added to the reactor in batches, and the flow rate of the gas phase (nitrogen/steam) is 0.68-0.8m/s. Working temperature 250℃/300℃/350℃, working pressure 0.2MPa.

生物质焙烧装置现场图：

1-蒸汽锅炉，2-生物质进料罐，3-生物质 焙烧反应器，4-焙烧后生物炭收集器，5-旋风分离器，6-冷水循环机，7-冷凝器，8 -控制面板，9-加热器

Site diagram of biomass roasting device:

1-steam boiler, 2-biomass feed tank, 3-biomass roasting reactor, 4-roasted biochar collector, 5-cyclone separator, 6-cold water circulation machine, 7-condenser, 8-control Panel, 9-Heater