本公司专注于连续生产反应器设备的研发与制造，产品性能稳定、操作简便，适用于多种化学反应。我们致力于提供高效、安全的反应器设备，助力客户实现连续化、自动化的生产流程，提升生产效率。本文介绍了一些用于连续生产的反应器的不同类型，简要说明了生产规格和制造标准。

1.

中试多区水平流反应器用于乳品废水处理

Pilot-scale multi-removal horizontal flow reactor for dairy wastewater treatment

确认在配备MR和US装置的多段卧式厌氧反应器(HFAR)中处理乳制品废水和产气的效率。

图1： 中试多区水平流反应器（a）示意图，（b）现场图： 1——进水； 2——废水； 3—污泥再循环； 4—搅拌叶片； 5—隔热； 6—膜组件； 7——压力表； 8—沼渣； 9——齿轮电机； 10——取样口； GM——微波发生器； GU——超声波发生器。

Horizontal flow anaerobic reactor (HFAR) (a) schematic diagram, (b) photo. 1—influent; 2—effluent; 3—sludge recirculation; 4—mixing blade; 5—thermal insulation; 6—membrane module; 7—gas meter; 8—digestate; 9—gearmotor; 10—sampling port; GM—microwave generator; GU—ultrasonic generator.

设计参数：总长度—4.0 m，总直径—0.3 m，总截面积—0.070 m²，工作截面积—0.063 m²，填充高度—0.25 m，总体积—0.28 m³ ，工作体积—0.25 m³

The HFAR design parameters were as follows: total length—4.0 m, total diameter—0.3 m, total cross-sectional area—0.070 m² , working cross-sectional area—0.063 m² , height of filling—0.25 m, total volume—0.28 m³ , working volume—0.25 m³.

图 2. 反应器设备 (a) 微波发生器，(b) 超声波发生器

使用微波发生器 (GM)（等离子）和磁控管加热反应器（图 2a），温度保持在38℃，当温度低于38℃时，微波发生器自动启动。

研究中使用的超声波发生器 (GU) 安装在 HFAR 的每个区域（图 2b）。各区域配备了四个超声波换能器，频率为 20 kHz，功率为 95 W。每个 GU 都集成了一个控制面板来控制其工作。

在中试多区水平流反应器HFAR上部，各工段均设有底物补充、污泥、沼气收集以及温度和pH测量的端口，这为HFAR各工段废水投加、厌氧污泥再循环和沼气分析提供了可能。

水力停留时间(HRT)为24小时。每个系列的持续 30 天，允许反应器内容物交换 30 倍。

 The reactor was heated using microwave generators (GM), (Plasmotomies) with magnetrons (Figure 2a).The temperature was maintained at 38 ℃, and when it dropped below, the microwave generators automatically started.

The ultrasonic generators (GU) used in the study were installed at each section of the HFAR (Figure 2b). Sections were equipped with a package of the four ultrasonic transducers with a frequency of 20 kHz and a power of 95 W. Each GU was integrated with a control panel to control its work.

In the upper part of HFAR, in all sections, there were ports for substrate supplementation, sludge, and biogas collection, as well as the temperature and pH measurement, which created the possibility of wastewater dosing to the various sections of HFAR, anaerobic sludge recirculation, and biogas analyzing.

The sludge from the bottom of the thickener was recycled and then mixed with the raw wastewater. Effluent was discharged outside the technological system.

2.

卧式螺杆反应器用于处理石墨废物

Horizontal screw reactor for treatment of graphite waste

卧式螺杆反应器是一种重要的化学反应设备，广泛应用于化工、制药、食品等领域。其核心部件是内部的螺杆结构，通过螺杆的旋转来推动物料进行混合和反应。

Horizontal screw reactor is an important chemical reaction equipment widely used in fields such as chemical, pharmaceutical, and food. The core component is the internal screw structure, which drives the mixing and reaction of materials through the rotation of the screw.

卧式螺杆反应器通过气化石墨颗粒表面上的放射性碳以及石墨基体的一部分来净化放射性石墨废物。

The horizontal screw reactor purifies the radioactive graphite waste by gasifying the radioactive carbon on the surface of the graphite particles and part of the graphite matrix.

图 1. (a) 卧式螺杆反应器示意图。 (b) 卧式螺杆反应器尺寸

Figure 1. (a) Schematic diagram of the horizontal screw reactor. (b) Dimensions of the Horizontal screw reactor.

卧式螺杆反应器具有由隔热材料体分开的三个加热区和单个旋转螺杆，可热气化在 373 K 下干燥的石墨颗粒。反应器长度 L、反应器管直径 D 和螺距 Lp 分别为 0.5、0.022 和 0.016m。

The screw reactor has three heating zones separated by insulators and a single revolving screw that thermally gasifies graphite particles dried at 373 K. The reactor length L, the reactor tube diameter D, and the screw thread pitch Lp, are 0.5, 0.022, and 0.016 m, respectively. 

类似产品图片如下所示：

3.

连续流反应器用于有机合成

Application of continuous flow reactor in Organic Synthesis

连续流反应器在有机合成中发挥着重要作用。其高效的传质传热性能、可控的反应条件以及快速连续的生产方式，使得有机合成反应更为精确、高效。同时，其绿色环保的特性也符合现代化学工业的发展需求，为有机合成领域带来革命性的变革。

图1：羰基化合物和金属有机试剂的反应

Figure I: A carbonyl compound and a metallo-organic reagent form a product

如图所示，两种原料经泵进入连续流反应器中，此外还有一个泵用于对系统进行溶剂清洗。连续流反应器由10个混合装置组成，每个装置包含2 x 16个40 x 220m的通道。

As shown in the figure, two raw materials are pumped into the continuous flow reactor, and there is also a pump for solvent cleaning of the system. The continuous flow reactor consists of 10 mixing devices, each containing 2x16 40x220m channels.

图2：用于微反应器实验室规模试验的设备

Figure 2: The equipment for lab-scale trials with the microreactor

图 4：羰基化合物和金属有机反应物的现场图

Figure 4: Scene diagram of the carbonyl compound and of the metallo-organic reactant

表 1：各种反应器类型和所选参数的结果

4.

新型三相催化浆料反应器

A new three-phase catalytic slurry reactor.

新型三相催化浆料反应器是一种先进的化工设备，结合了催化反应与浆料处理的双重功能。它采用独特的三相催化技术，能够实现高效、稳定的化学反应，同时处理含有固体颗粒的浆料。该反应器具有结构紧凑、操作简便、传热传质效果好等优点，可广泛应用于石油化工、精细化工等领域，为工业生产提供强有力的技术支持。

图1. 新型反应器实图

Fig. 1. The real diagram of the new reactor

图 2. 邻甲酚氢化为邻甲基环己醇

Fig. 2. Hydrogenation of ortho cresol to ortho methyl-cyclohexanol.

该反应器是一个长度为 L、内径为 D 的圆柱形反应器，配有纵向轴，其上安装有多个搅拌翼。最大搅拌速度为1500 rpm。最佳内径在 40 至 60 毫米之间，测试反应器的典型长度在 200 至 800 毫米之间。

This reactor is a cylindrical reactor of length L and internal diameter D equipped with a longitudinal shaft on which are mounted several impellers. Maximal agitation speed is 1500 rpm. Optimal internal diameter has to be between 40 and 60 mm. Typical length of the tested reactors is between 200 and 800 mm.

具有商业规模生产能力的典型应用

5.

新型反应器用于Buchwald−Hartwig 胺化连续生产工艺

New reactor used in Buchwald-Hartwig amination continuous production process

 反应器在Buchwald−Hartwig胺化连续生产工艺中发挥着关键作用。其高效传热传质特性确保了反应条件的精准控制，从而实现了胺化反应的高效进行。连续生产工艺的应用不仅提高了生产效率，还降低了生产成本，使得Buchwald−Hartwig胺化反应在工业化生产中具有更广阔的应用前景。

方案 1. Buchwald−Hartwig 胺化反应

Scheme 1. Buchwald−Hartwig Amination Reaction

图 2. 工艺流程：固体分离、水处理和相分离

Figure 2. Process flow: solid separation, aqueous workup and phase split

图 3. 双进料连续流微反应器示意图

注射器 1：PhMe 中的预催化剂；注射器 2：ArBr、NMP、KOtAm、4,4'-二叔丁基苯（内标）的 PhMe 溶液。

Figure 3. Schematic of the two-feed continuous flow microreactor.

Syringe 1: Precatalyst in PhMe; Syringe 2: ArBr, NMP, KOtAm, 4,4′-di-tert-butylbiphenyl (internal standard) in PhMe.

连续流反应器的组装如图 3 所示，包括内径 2 mm 不锈钢管的 T 型混合器和两个提供试剂进料的注射器。

Our continuous flow microreactor was assembled as shown in Figure 3 and consisted of a T-mixer linked to a stainless steel tube with an internal diameter of 2 mm, with two syringes providing the reagent feeds.

图4.实验室规模的流动和催化剂回收实验系统示意图，初始流和反应器浓度表

Figure 4. Schematic diagram of the lab-scale flow and catalyst recycling experimental system and table of initial stream and reactor concentrations.

这个装置设计有三个独立的区域，使得碱和催化剂在混合之前能够与其他化学试剂分开。每个流程中的原料（如图4）都被保存在配有磁力搅拌器的玻璃容器中。一个由聚四氟乙烯制成的盘管反应器（容量为10.9毫升，内径为1.5毫米）被放置在设定为70°C的超声波浴中。当反应完成后，产物流通过醋酸水溶液（pH值约为5.5）进行冷却。随后，进行相分离，有机相被引导回A流进料容器。在这里，它与新的催化剂混合，然后再次进行反应。这个循环过程导致A流进料的有机相被稀释（见图4的示意图）。

For this set up, three separate streams were employed, keeping the base and catalyst separate from the other reagents prior to the mixer. The feeds for the three streams (see Figure 4) were kept in magnetically stirred glass vessels, and the PTFE coil reactor (10.9 mL volume and 1.5 mm internal diameter) was placed into an ultrasonic bath at 70 °C to avoid tube clogging by surface crystallization of the potassium bromide byproduct. Post reaction, the product stream was quenched with an aqueous acetic acid stream at around pH 5.5 and was observed to give the predicted separation of the starting material and catalyst in the organic phase from the acetic acid salt of the product in the aqueous phase. After phase separation the organic phase was returned to the Stream A feed vessel and mixed with the fresh catalyst. This recycle of the separated organic phase post reaction consequently dilutes the Stream A feed .

图5.新反应堆装置的简化工艺流程图

Figure 5. Simplified process flow diagram for the new reactor unit.

6.

多级反应器用于连续液液相反应

Multistage reactors for continuous liquid-liquid phase reactions

多级反应器在连续液液相反应中扮演着至关重要的角色。其多级设计使得反应物在不同的反应阶段中能够经历不同的反应条件，从而有效提高反应的转化率和产物选择性。此外，多级反应器通常具有优异的传质传热性能，这有助于反应的高效进行。因此，在连续液液相反应中，多级反应器能够实现更高效、更稳定的反应过程，提升产品质量和生产效率。

图1反应器塔示意图

Fig. 1 Schematic drawing of the reactor column

如图1所示：双夹套哈氏合金小型反应器塔（额定压力高达 40 bar），两相通过塔底部入口处的 T 形件泵送，混合物通过一个小开口在塔的每个区域（或室）之间流动，转化率随着每个连续阶段的增加而增加，反应时间（在柱中的停留时间）是通过进料的流速来控制的。

As shown in Figure 1: Double-jacketed Hastelloy small reactor column (rated pressure up to 40bar), the two phases are pumped through a T-shaped piece at the inlet at the bottom of the column, and the mixture passes through a small opening in each area of the column (or chambers) so that the conversion increases with each successive stage, and the reaction time (residence time in the column) is controlled by the flow rate of the feed.

图2带有顶置搅拌器(a，b)和搅拌器(C)的反应器

Fig. 2 Reactor column with overhead stirrer (a, b) and inserts (c).

搅拌器固定腔室直径28 毫米，每个阶段的体区间的高度/直径为(0.6)固定比率，根据流量确定13个室，这些隔板安装在三个垂直支架上，这些支架也充当挡板。一系列叶轮安装在穿过板中心的轴上，并连接到磁耦合高压顶置搅拌器，确保了每个阶段的高效混合（图 2）

The stirrer has a fixed chamber diameter of 28 mm and a fixed ratio of height/diameter of the body sections of each stage (0.6). There are 13 chambers determined according to the flow rate. These partitions are mounted on three vertical brackets that also act as baffles. . A series of impellers mounted on a shaft through the center of the plate and connected to a magnetically coupled high-pressure overhead stirrer ensure efficient mixing at every stage (Figure 2).

图3(A)单级和级间管(1 mm、2 mm和3 mm)；(B)分散相液滴尺寸与管口尺寸的示意图。

Fig. 3 (a) Single stage and tube between the stages (1, 2, and 3 mm); (b) schematic representation of droplet size of dispersed phase vs. tube opening size.

方案2 化合物3的连续流动制备

Scheme 2: Continuous flow preparation of compound 3.

用于发生反应的装置包括三个连续注射泵、每个泵的压力传感器、加热/冷却系统和背压调节器 。该设置由件控制，该软件允许设置安全范围以及在线监测反应条件，例如流速、温度和压力。

The setup used to perform the reaction comprised three continuous syringe pumps, a pressure sensor for each pump, a heating/cooling system and a back-pressure regulator. The setup was controlled by software that allowed the setting of safety ranges as well as the online monitoring of reaction conditions such as flow rates, temperature and pressure.

7.

连续流反应器用于光催化反应

Continuous flow reactor for photocatalytic reactions

连续流反应器在光催化反应中展现出优异的应用价值。这种反应器能够高效地将光催化剂与反应物相结合，在光照条件下促进反应的进行。由于连续流反应器具有优异的传质传热性能，能够确保反应过程中温度、压力等参数的精准控制，从而优化反应条件，提高反应效率。此外，连续流反应器还能够实现反应物的连续输入和产物的连续输出，使得光催化反应过程更为高效、连续和可控。这有助于减少反应过程中的副产物生成，提高产物的纯度和收率。

图1. A) 外部光源定向照射的连续流光化学平台； B) 具有锥形热交换器作为毛细管稳定元件的光反应器。

Fig1. A) Continuous flow photochemistry platform with directional irradiation by an external light source; B) photoreactor with cone-shaped heat exchanger as stabilizing element for the capillary. 

毛细管（外径 1.59 毫米，内径 0.79 毫米）缠绕在锥体周围，并通过凹槽的空腔保持稳定（图 1）。锥体本身是中空的，可以用冷却剂连续冲洗，以维持毛细管内所需的温度。

The capillary (o.d. 1.59 mm, i.d. 0.79 mm) is wrapped around the cone and gets stabilized by the cavities of the groove (Fig 1). The cone itself is hollow and can be continuously flushed with a coolant to maintain the desired temperature inside the capillary.

图2.A）用于三相混合的悬浮给药装置（插图：气-液-固接触示意图）； B) 固体光催化剂在液相中产生的段塞流； C) 稳态条件下配备 SMBR 的 FEP 毛细管反应器。

Fig 2. A) Suspension dosing device for triphasic mixing (inset: schematic representation of gas-liquid-solid contacting); B) Resulting slug flow with solid photocatalyst in the liquid phase; C) FEP capillary reactor with SMBRs under steady state conditions.

氟化乙烯丙烯 (FEP)           fluorinated ethylene propylene (FEP)

图 3. A) 自制三层 FEP 毛细管光反应器，用于实验测定单独毛细管中的光子通量； B) 围绕中央汞灯的毛细管示意图

Fig 3. A) Self-made three-layer FEP capillary photoreactor used for the experimental determination of photon fluxes in separate capillaries; B) schematic representation of the capillaries wrapped around the central Hg lamp

图 5. A) 紧凑型两层毛细管光反应器，具有可更换的 LED 阵列以及独立的毛细管和 LED 冷却； B) 装配有 LED 阵列的光反应器，可发射 520 nm 的绿光； C) LED 阵列支架，便于轻松切换到其他发射波长。

Fig 5. A) Compact two-layer capillary photoreactor with exchangeable LED arrays and separate capillary and LED cooling; B) Assembled photoreactor with LED array for green light emission at 520 nm; C) Holder for LED arrays facilitating an easy switch to other emission wavelengths.

图 6. A) 芯直径为 20 μm 的 kagomé 空心 PCF 示意图； B) Kagomé 空心 PCF 的 SEM 图像； C) 以 PCF 作为 µL 规模微反应器的连续流设置示意图

Fig 6. A) Schematic representation of a kagomé hollow core PCF with a core diameter of 20 μm; B) SEM image of a kagomé hollow core PCF; C) Schematic representation of continuous flow setup with a PCF as microreactor on the μL scale

光子晶体光纤 (PCF)              photonic crystal fibers (PCFs)

图 7. A) 带有 LED 阵列、电机和控制箱的已拆卸涡流反应器； B) LED阵列和镜子分布在玻璃管周围； C) 涡流反应器的示意图，显示反应溶液的输送和去除以及气体入口； D) 和 E) 通过 CFD 建模并在实时运行中形成涡流。

Fig 7. A) Disassembled vortex reactor with LED arrays, motor and control box; B) LED arrays and mirror blocks assembled around the glass tube; C) Schematic representation of the vortex reactor showing delivery and removal of reaction solution and gas intake; D) and E) Vortices formation as modelled via CFD and in live operation.

图 8.A) 具有 32 个微通道的不锈钢 FFMR 反应板（宽度：600 μm，深度：200 μm）。； B) 微通道降膜法示意图：(S) 不锈钢微通道反应板，(L) 液膜，(G) 气室，(W) 微通道宽度和(H) 高度，(δl) 液膜高度(δg) 气室高度

Fig 8. A) Stainless steel FFMR reaction plate with 32 microchannels (width: 600 μm, depth: 200 μm); B) Schematic representation of the falling film approach for microchannels: (S) stainless steel microchannel reaction plate, (L) liquid film, (G) gas chamber, (W) microchannel width and (H) height, (δl ) liquid film height and (δg) gas chamber height.

8.

含固相多腔室微反应器

Solid-phase multi-chamber microreactor

图 1 微型 CSTR 级联设计示意图。 (a) CAD 图中所示的单级 CSTR 以及实际产品的三个主要部件。 (b) 多个 CSTR 串联在铝支架上。上图中的白色比例尺为 10 毫米。

Fig. 1 Sketch of the miniature CSTR cascade design. (a) The singlestage CSTR shown in CAD drawing, and the three main components of the actual product. (b) Multiple CSTRs in series on an aluminium holder. The white scale bars in the pictures above are 10 mm.

 氟化乙烯共聚物（FEP）       Fluorinated ethylene propylene（FEP）

反应器设计单个CSTR装置由三个主要部件组成，包括聚四氟乙烯（PTFE）反应器块、耐热玻璃盖和不锈钢盖（图1a）。

PTFE反应器为30mm×30mm的方形块，厚度为19mm。圆筒形内室的直径为18毫米，深度为10毫米。 O 形环间隙围绕着带有硅胶芯的 1/16 英寸 FEP O 形环的腔室。玻璃盖为耐热硼硅酸盐玻璃，尺寸为30 mm × 30 mm × 4.8 mm。不锈钢盖采用超耐腐蚀316不锈钢，尺寸为30毫米×30毫米×3.2毫米。所有挤压二维形状均采用水射流加工制造。除了 2D 形状外，反应室和 O 形环间隙还使用数控铣削进行加工。多个 CSTR 单元安装在铝制支架上（图 1b）。铝制支架 (150 mm × 70 mm × 3.2 mm) 最多可容纳 8 个 CSTR。所有连接端口均具有1/4-28螺纹，可使用常见的配件直接连接。两个 CSTR 使用外部带有 1/4-28 螺纹的管连接。

Reactor design A single CSTR unit consists of three main components, including a polytetrafluoroethylene (PTFE) reactor block, a heat-resistant glass cover and a stainless steel cover (Fig. 1a).

The PTFE reactor is a 30 mm × 30 mm square block with a thickness of 19 mm. The cylinder-shaped inner chamber has a diameter of 18 mm and a depth of 10 mm. An O-ring gap surrounds the chamber for the 1/16′′ FEP O-ring with a silicone core. The glass cover is heat-resistant borosilicate glass with dimensions of 30 mm × 30 mm × 4.8 mm. The stainless steel cover is super-corrosion-resistant 316 stainless steel with dimensions of 30 mm × 30 mm × 3.2 mm. All extruded 2D shapes were fabricated using water jet machining. In addition to 2D shapes, the reactor chamber and the O-ring gap were machined using CNC milling. Multiple CSTR units are mounted on an aluminum holder (Fig. 1b). The aluminum holder (150 mm × 70 mm × 3.2 mm) can hold up to 8 CSTRs. All connection ports have 1/4-28 threads, which can be directly connected using common fittings. Two CSTRs are connected using a tube with 1/4-28 thread outside.

图 2 使用在线 UV-Vis 记录入口和出口浓度分布的停留时间分布测量方案。

Fig. 2 Scheme of the residence time distribution measurement using in-line UV-Vis to record concentration profiles at the inlet and outlet.

图3 CSTR级联运行过程照片，固体分数沿流动方向增加（白色箭头g为重力方向）

Fig.3 Photograph of the CSTR cascade during the operation showing the solid fraction increasing along the flow direction (the white arrow marked g shows the direction of gravity）

9.

含固相的连续搅拌反应器用于光催化反应

Continuously stirred reactor containing solid phase for photocatalytic reactions

如图 1 所示为：用于处理含固相的连续搅拌反应器的爆炸视图CAD模型，从上到下，依次为上铝盖、Pyrex 玻璃窗、第二个铝盖、包含五个 CSTR 室的聚四氟乙烯 (PTFE) 反应器块以及铝制外壳

As shown in Figure 1, an exploded view CAD model is used to process a continuous stirred reactor containing solid phases. From top to bottom, it sequentially contains the upper aluminum co ver, Pyrex glass window, second aluminum cover, polytetrafluoroethylene (PTFE) reactor block containing five CSTR chambers, and the aluminum housing。

图 2 (a)光催化连续搅拌反应器平台示意图，包括浆料泵、CSTR 级联、3 个 LED 光源 (440 nm)、聚焦透镜和加压馏分收集器（b ) 灯和反应器的图像

Figure 2 (a) Schematic of the photo-CSTR platform including the slurry pump, CSTR cascade, 3 LED light sources (440 nm), focusing lenses and the pressurized fraction collector (b) Image of the lamps and reactor.

所有起始材料都可以通过浆料泵送入 photo-CSTR（图 2a）。为了利用重力来增强固体输送并最大程度地减少堵塞，渣浆泵位于 CSTR 上方约 300 毫米处。该系统通过加压馏分收集器加压，其中 10 psig 氩气直接施加到收集室，以防止反应器中气体逸出（图 2b）。

We designed the platform where all starting materials can be fed into the photo-CSTR via the slurry pump (Figure 2a). With the intention to use gravity to enhance solid transport and minimize clogging, the slurry pump is positioned ~300 mm above the CSTR. The system is pressurized via a pressurized fraction collector, where 10 psig argon is applied directly to the collection chamber to prevent gas evolution in the reactor (Figure 2b).  

10.

连续振荡挡板反应器用于连续生产扑热息痛

Reactive Crystallization of Paracetamol in a Continuous Oscillatory Baffled Reactor

图 1. 照片显示 COBR 设置（T1−T6，六个热电偶；AA，乙酸酐；4-AP，4-氨基苯酚）

Fig 1. Photograph showing the COBR setup (T1−T6, six thermocouples; AA, acetic anhydride; 4-AP, 4-aminophenol).

在连续振荡挡板反应器中成功进行的扑热息痛反应种子冷却结晶。连续振荡挡板反应器（反应器规格DN15）由 11 根夹套折流直管和 6 根无夹套弯管组成，并用热套管包裹以减少热量损失。 总长度和体积分别为 9.5 m 和 1.68 L。

Successful paracetamol reaction seed cooling crystallization in a continuously oscillating baffle reactor.The continuous oscillating baffle reactor (reactor specification DN15) consists of 11 jacketed baffled straight tubes and 6 unjacketed bent tubes, and is wrapped with a thermowell to reduce heat loss. The total length and volume are 9.5m and 1.68L respectively.

 图 2. 对乙酰氨基酚反应性晶种冷却结晶的 COBR 平台示意图（T1−T6，六个热电偶；AA，乙酸酐；4-AP，4-氨基苯酚）

Figure 2. Schematic of the COBR platform for the reactive seeded cooling crystallization of paracetamol (T1−T6, six thermocouples; AA, acetic anhydride; 4-AP, 4-aminophenol).

水通过三个水浴 (GP 200) 在预设温度下循环通过 COBR 夹套，以建立用于反应和结晶的三个温度区（在图 2 中显示为不同的颜色和线宽）。采用六个热电偶（图 2 中的 T1−T6）来记录操作的温度曲线。通过单独的水浴控制和维持种子悬浮液的温度以达到所需的过饱和度。连接种子悬浮液与 COBR 的管道经过适当隔热，以确保正确的给料温度。

Water was circulated through the jackets of the COBR at preset temperatures by three water baths (GP 200) in order to establish three temperature zones (shown as different colors and line widths in Figure 2) for reaction and crystallization. Six thermocouples (T1−T6 in Figure 2) were employed to record the temperature profiles of the operation. The temperature of seed suspension was controlled and maintained by a separate water bath to achieve the required supersaturation. The tubing connecting the seed suspension with the COBR was properly insulated to ensure the correct seeding temperature.

本公司致力于连续流生产反应器设备的研发与制造，产品性能优良、使用安全快捷，适用于多种化学反应，助力客户实现连续化、自动化的生产流程，提升生产效率，节约运营成本。